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HRID 622469作成日:2026年10月27日

Cyanuric chloride → 2,4-Dichloro-6-methoxy-3,5-triazine

https://huagongshe.com/reaction/622469

反応式

関与物質

役割名称HCID仕込み量
反応物Cyanuric chlorideHCID 7954—
反応物Sodium BicarbonateHCID 516892—
溶媒MethanolHCID 887—
生成物2,4-Dichloro-6-methoxy-3,5-triazineHCID 19267—

反応条件

温度0 °C

反応手順

7 parts of sodium hydrogencarbonate was added to 50 parts of methanol. This mixture was cooled to 0° C. from outside. Then, 15 parts of cyanuric chloride was added to conduct a reaction for 60 minutes (First condensation). To the reaction mixture was added 100 parts of ice water, and the crystal precipitated was collected by filtration to obtain 2-methoxy-4,6-dichloro-1,3,5-triazine.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04771132
出典データセットuspto-grants-1988_09
ORD IDord-746073f0754f43e5a068c64e1aa9eb68
出典メモuspto-grants-1988_09