関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Cyanuric chloride | HCID 7954 | — |
| 反応物 | Sodium Bicarbonate | HCID 516892 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 2,4-Dichloro-6-methoxy-3,5-triazine | HCID 19267 | — |
反応手順
7 parts of sodium hydrogencarbonate was added to 50 parts of methanol. This mixture was cooled to 0° C. from outside. Then, 15 parts of cyanuric chloride was added to conduct a reaction for 60 minutes (First condensation). To the reaction mixture was added 100 parts of ice water, and the crystal precipitated was collected by filtration to obtain 2-methoxy-4,6-dichloro-1,3,5-triazine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04771132 |
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| 出典データセット | uspto-grants-1988_09 |
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| ORD ID | ord-746073f0754f43e5a068c64e1aa9eb68 |
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| 出典メモ | uspto-grants-1988_09 |
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