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N-Methylmethanesulfonamide → 1-(2-amino-5-methoxyphenyl)-2-(N-methylsulphamoyl)ethanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-Methylmethanesulfonamide | HCID 97632 | — |
| 反応物 | Ethyl 2-amino-5-methoxybenzoate | HCID 21291483 | — |
| 反応物 | Butyllithium | HCID 178418339 | — |
| 生成物 | 1-(2-amino-5-methoxyphenyl)-2-(N-methylsulphamoyl)ethanone | HCID 21291480 | — |
反応手順
In a similar manner to that described in Example 12(a), N-methylmethanesulphonamide was reacted with n-butyl lithium and the product was reacted with ethyl 2-amino-5-methoxybenzoate to give the novel compound 1-(2-amino-5-methoxyphenyl)-2-(N-methylsulphamoyl)ethanone, m.p. 117°-118°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04772614 |
| 出典データセット | uspto-grants-1988_09 |
| ORD ID | ord-c033204fb9e5461cb0f31c74c1345012 |
| 出典メモ | uspto-grants-1988_09 |