化工社化工社 化学情報印刷レポート · 研究参考用
N-Methylmethanesulfonamide → 1-(4-fluoro-2-methylaminophenyl)-2-(N-methylsulphamoyl)ethanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-Methylmethanesulfonamide | HCID 97632 | — |
| 反応物 | Methyl 4-fluoro-2-(methylamino)benzoate | HCID 13474393 | — |
| 反応物 | Butyllithium | HCID 178418339 | — |
| 生成物 | 1-(4-fluoro-2-methylaminophenyl)-2-(N-methylsulphamoyl)ethanone | HCID 21291484 | — |
反応手順
In a similar manner to that described in Example 12(a), N-methylmethanesulphonamide was reacted with n-butyl lithium and the product reacted with methyl 4-fluoro-2-methylaminobenzoate to give the novel compound 1-(4-fluoro-2-methylaminophenyl)-2-(N-methylsulphamoyl)ethanone, m.p. 140°-142°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04772614 |
| 出典データセット | uspto-grants-1988_09 |
| ORD ID | ord-63e621efc46e492b838d0e66c85af94a |
| 出典メモ | uspto-grants-1988_09 |