化工社化工社 化学情報印刷レポート · 研究参考用
Cyclohexane → Spiro[cyclohexane-1,9'-fluorene]
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexane | HCID 8078 | — |
| 触媒 | HCID 178503044 | HCID 178503044 | — |
| 生成物 | Spiro[cyclohexane-1,9'-fluorene] | HCID 12861606 | — |
反応手順
110 g of spiro[cyclohexane-1,9'-fluorene] obtained in the above (1), 100 ml of cyclohexane solvent and 20 g of 5% ruthenium-carbon catalyst (manufactured by Japan Engelhard Co.) were charged in an autoclave of 1 liter and hydrogenation was effected with a hydrogen pressure of 80 kg/cm2G at 170° C. for 5 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04774013 |
| 出典データセット | uspto-grants-1988_09 |
| ORD ID | ord-898e96dc55a24a45876203d87c37ab65 |
| 出典メモ | uspto-grants-1988_09 |