Thiophenol → Diphenyl sulfide

HRID 623238

反応式

HRID 623238 の反応式
[C:1]1([SH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>C1(C)C=CC=CC=1>[C:1]1([S:7][C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

参加物

3

反応物 1

HCID 7969Thiophenol

生成物 1

HCID 8766Diphenyl sulfide

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

A mixture of bis(dineophyl-orthotrifluoromethylphenyltin)oxide (6.0 g, 5.6 mmol) prepared in Example 6, thiophenol (1.2 g, 11.2 mmol) and toluene (40 g) was treated with the procedure described in Example 7. The product was recrystallized from n-hexane to obtain 5.2 g of dineophylorthotrifluoromethylphenyltin phenylsulfide as a white solid.

後処理

  1. additionwas treated with the procedure
  2. customThe product was recrystallized from n-hexane

出典と根拠

ORDレコード
ord-7087eac787814b4481a45eda5fa3f06b
出典データセット
uspto-grants-1988_09
特許番号
US04774235

関連ノート

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