Thiophenol → Diphenyl sulfide
反応式
[C:1]1([SH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>C1(C)C=CC=CC=1>[C:1]1([S:7][C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1参加物
3
試薬・触媒・溶媒 1
実験手順
A mixture of bis(dineophyl-orthotrifluoromethylphenyltin)oxide (6.0 g, 5.6 mmol) prepared in Example 6, thiophenol (1.2 g, 11.2 mmol) and toluene (40 g) was treated with the procedure described in Example 7. The product was recrystallized from n-hexane to obtain 5.2 g of dineophylorthotrifluoromethylphenyltin phenylsulfide as a white solid.
後処理
- additionwas treated with the procedure
- customThe product was recrystallized from n-hexane
出典と根拠
- ORDレコード
- ord-7087eac787814b4481a45eda5fa3f06b
- 出典データセット
- uspto-grants-1988_09
- 特許番号
- US04774235
反応ノート
読み込み中…