6-Methoxy-1H-indole → 3-(2-bromoethyl)-6-methoxy-1H-indole
反応式
[Br:1][CH2:2][CH2:3][C:4]1[C:12]2[C:7](=[CH:8][CH:9]=[C:10](OC)[CH:11]=2)[NH:6][CH:5]=1.[CH3:15][O:16]C1C=C2C(C=CN2)=CC=1>>[Br:1][CH2:2][CH2:3][C:4]1[C:12]2[C:7](=[CH:8][C:9]([O:16][CH3:15])=[CH:10][CH:11]=2)[NH:6][CH:5]=1参加物
3
実験手順
The title compound was synthesized according to above mentioned procedure for 3-(2-bromoethyl)-5-methoxy-1H-indole, starting with 6-methoxyindole yielding a brown oil which was stored in the freezer. LC-MS conditions B: tR=0.81 min, [M+H]+=254.13.
出典と根拠
- ORDレコード
- ord-af94cd4df54d4c02ab77e2b12c24e8e2
- 出典データセット
- uspto-grants-2016_04
- 特許番号
- US09303023B2
反応ノート
読み込み中…