化工社化工社 化学情報印刷レポート · 研究参考用
Tetrahydrofurfuryl alcohol → 6-((Tetrahydrofuran-2-yl)methoxy)-5-(trifluoromethyl)picolinic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tetrahydrofurfuryl alcohol | HCID 7360 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 6-Chloro-5-(trifluoromethyl)picolinic acid | HCID 70701016 | — |
| 生成物 | 6-((Tetrahydrofuran-2-yl)methoxy)-5-(trifluoromethyl)picolinic acid | HCID 71087646 | — |
反応手順
In analogy to the procedure described in Example 4 a), 6-chloro-5-(trifluoromethyl)picolinic acid (CAN 855915-21-8) was reacted with (tetrahydrofuran-2-yl)methanol (CAN 97-99-4) in the presence of potassium hydroxide to yield the title compound as yellow solid; MS (EI): m/e=290.0 [MH+].
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09303012B2 |
| 出典データセット | uspto-grants-2016_04 |
| ORD ID | ord-36267bffa0e54c9aab12d608f074bb6f |
| 出典メモ | uspto-grants-2016_04 |