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HRID 625174作成日:2026年10月26日

2-[(2-Nitrophenyl)sulfanyl]benzoic acid → 2-((2-Aminophenyl)thio)benzoic acid

https://huagongshe.com/reaction/625174

反応式

関与物質

役割名称HCID仕込み量
反応物2-[(2-Nitrophenyl)sulfanyl]benzoic acidHCID 376978—
触媒PalladiumHCID 23938—
溶媒Ethyl AcetateHCID 8857—
生成物2-((2-Aminophenyl)thio)benzoic acidHCID 10955828—

反応手順

To a solution of 2-((2-nitrophenyl)thio)benzoic acid, prepared as described in the previous step, (43.3 g, 0.157 mol) in ethyl acetate (500 mL) was added Pd/C (8 g). The reaction solution was stirred at room temperature overnight under hydrogen gas atmosphere. The mixture was filtered and concentrated to provide the title compound.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09304126B2
出典データセットuspto-grants-2016_04
ORD IDord-91e47b447afe49b2be3082fc09c284fa
出典メモuspto-grants-2016_04