Napropamide-M → Napropamide

HRID 625664

反応式

HRID 625664 の反応式
[CH3:1][C:2]([CH3:4])=[O:3].[OH2:5].[CH3:6][CH2:7][N:8]([C:11]([C@H:13]([O:15][C:16]1[C:25]2[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=2)[CH:19]=[CH:18][CH:17]=1)[CH3:14])=[O:12])[CH2:9][CH3:10]>O.CC(C)=O>[CH3:10][CH2:9][N:8]([C:11]([CH:13]([O:15][C:16]1[CH:17]=[CH:18][CH:19]=[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:25]=12)[CH3:14])=[O:12])[CH2:7][CH3:6].[CH3:6][CH2:7][N:8]([C:1]([C@H:2]([O:3][C:21]1[C:20]2[C:25](=[CH:16][CH:17]=[CH:18][CH:19]=2)[CH:24]=[CH:23][CH:22]=1)[CH3:4])=[O:5])[CH2:9][CH3:10]

参加物

6

反応物 2

HCID 13013865Napropamide-MHCID 18366337Propan-2-one--water (1/1)

生成物 2

HCID 27189NapropamideHCID 13013865Napropamide-M

試薬・触媒・溶媒 2

HCID 180Acetone溶媒HCID 962Water溶媒2 回

実験手順

The highest concentration of Napropamide was prepared by measuring a calculated volume by weight and diluting with tap water to the full required volume. Lower concentrations were prepared by serial dilution with water. D-Napropamide was prepared by dissolving the calculated weight in acetone and adding water to give the full required volume in 50:50 acetone+water. Lower concentrations were prepared by serial dilution with 50:50 acetone+water. D-Napropamide dissolved completely.

後処理

  1. concentrationLower concentrations
  2. customwere prepared by serial dilution with water
  3. concentrationLower concentrations
  4. customwere prepared by serial dilution with 50:50 acetone+water

出典と根拠

ORDレコード
ord-69a51dde74d642728b78d94dbc91b910
出典データセット
uspto-grants-2016_04
特許番号
US09307765B2

関連ノート

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