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HRID 62568作成日:2026年10月26日

Glucaric Acid → Adipic Acid

https://huagongshe.com/reaction/62568

反応式

関与物質

役割名称HCID仕込み量
反応物Glucaric AcidHCID 33037—
反応物Galactaric acidHCID 3037582—
触媒RheniumHCID 23947—
生成物Adipic AcidHCID 196—

反応手順

Further, as described above, the starting material (glucaric acid or galactaric acid), rhenium catalyst, and acid catalyst are added to the reaction solvent, and reacted together at a proper temperature for a proper reaction time, then separated and purified with a conventional method (e.g., purification with silica column) to obtain glucaric acid ester or galactaric acid ester as an intermediate of adipic acid. In one embodiment, the reaction temperature ranges from 100 to 200° C., and the reaction time is 12 to 24 hours.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09447012B2
出典データセットuspto-grants-2016_09
ORD IDord-e4d92eb81e1047428d952ffc9a9ab295
出典メモuspto-grants-2016_09