Hydrochloric Acid → 1-(4-Bromophenyl)ethylamine hydrochloride

HRID 626400ノート

反応式

HRID 626400 の反応式
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C@@H:8]([NH:10][S@](C(C)(C)C)=O)[CH3:9])=[CH:4][CH:3]=1.[ClH:17]>CO>[ClH:17].[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C@@H:8]([NH2:10])[CH3:9])=[CH:4][CH:3]=1

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 86732639HCID 86732639、化合物

生成物 1

HCID 534848701-(4-Bromophenyl)ethylamine hydrochloride

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

(S)—N—((S)-1-(4-bromophenyl)ethyl)-2-methylpropane-2-sulfinamide (170 mg, 0.56 mmol) was dissolved in methanol (2 mL) followed by addition of con.HCl (1 mL). The mixture was stirred at RT for 4 h and then was concentrated and evaporated with toluene twice to afford the titled compound.

後処理

  1. additionfollowed by addition of con
  2. concentrationwas concentrated
  3. customevaporated with toluene twice

出典と根拠

ORDレコード
ord-2c4a12918ec54afba31feacce594bbd3
出典データセット
uspto-grants-2016_04
特許番号
US09309227B2

反応ノート

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