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3-Bromopentane → 2-Chloro-1-ethoxy-5-iodo-3-(pentan-3-yloxy)benzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Bromopentane | HCID 15738 | — |
| 反応物 | 2-Chloro-3-ethoxy-5-iodophenol | HCID 67042212 | — |
| 生成物 | 2-Chloro-1-ethoxy-5-iodo-3-(pentan-3-yloxy)benzene | HCID 67041812 | 79% |
反応手順
2-Chloro-1-ethoxy-5-iodo-3-(pentan-3-yloxy)benzene (8) (1.2 g, 79%) was prepared from 2-chloro-3-ethoxy-5-iodophenol (7) (1.1 g, 3.7 mmol) using a procedure essentially the same as in step (i) for AAA-001 except that 3-bromopentane was used instead of cyclopentyl bromide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09447028B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-8181d3479b6a417fa4adc534e9103e2d |
| 出典メモ | uspto-grants-2016_09 |