化工社化工社 化学情報印刷レポート · 研究参考用
2-Propanethiol → 2-Isopropylsulfanyl-pyrimidine-4-carboxylic acid ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Propanethiol | HCID 6364 | — |
| 反応物 | Ethyl 2-chloropyrimidine-4-carboxylate | HCID 22509306 | — |
| 生成物 | 2-Isopropylsulfanyl-pyrimidine-4-carboxylic acid ethyl ester | HCID 90118331 | 68% |
反応手順
2-Chloropyrimidine-4-carboxylic acid ethyl ester (0.024 g, 0.13 mmol) obtained in Step A and 2-propanethiol were reacted in the same manner as in Step A of Preparation Example 16 to obtain the title compound (0.02 g, 68%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09447044B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-bb76834c5a184a2880af0b5f4d64a1de |
| 出典メモ | uspto-grants-2016_09 |