化工社化工社 化学情報印刷レポート · 研究参考用
Phthalic Anhydride → Dinonyl phthalate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phthalic Anhydride | HCID 6811 | — |
| 反応物 | 1-Nonanol | HCID 8914 | — |
| 触媒 | Methanesulfonic Acid | HCID 6395 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Dinonyl phthalate | HCID 6787 | 103.4% |
反応手順
567 g of nonyl alcohol produced in Example 1 was combined with 280 g of phthalic anhydride, 200 g of toluene and 5.5 g of methanesulfonic acid. The reaction was set up for reflux through a Dean-Stark trap using a nitrogen purge and slow stiffing. The reactor contents were refluxed for 5 hours. Residual catalyst was neutralized with a 10% NaCO3 solution and the product was water washed. The product was purified by vacuum stripping and distillation to yield 818 g of dinonyl phthalate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09315436B2 |
| 出典データセット | uspto-grants-2016_04 |
| ORD ID | ord-53c00a14720e44be9f8418de97e646eb |
| 出典メモ | uspto-grants-2016_04 |