化工社化工社 化学情報印刷レポート · 研究参考用
4-Hydroxybenzaldehyde → 4-(3-Methylbutoxy)benzaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Hydroxybenzaldehyde | HCID 126 | — |
| 反応物 | Sodium Iodide | HCID 5238 | — |
| 反応物 | 1-Iodo-3-methylbutane | HCID 10924 | — |
| 生成物 | 4-(3-Methylbutoxy)benzaldehyde | HCID 250101 | 92.6% |
反応手順
The compound was synthesized as in Example 24.1, using 4-hydroxybenzaldehyde (200 mg, 1.64 mmol) and 1-iodo-3-methylbutane (649 mg, 1.97 mmol) in place of 1-chloro-3,3-dimethylbutane (no sodium iodide was used) to give 4-(isopentyloxy)benzaldehyde (292 mg, quant. crude) as a dark yellow oil that was used without further purification or characterization.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09315495B2 |
| 出典データセット | uspto-grants-2016_04 |
| ORD ID | ord-11006f97bdad4ecd9c18c5ee4f5e5d47 |
| 出典メモ | uspto-grants-2016_04 |