化工社化工社 化学情報印刷レポート · 研究参考用
5-Bromothiophene-2-carbaldehyde → 5-Propylthiophene-2-carbaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Bromothiophene-2-carbaldehyde | HCID 78428 | — |
| 反応物 | 1-Propylboronic acid | HCID 351065 | — |
| 生成物 | 5-Propylthiophene-2-carbaldehyde | HCID 3159601 | 29% |
反応手順
The compound was synthesized as in Example 3.1 using 5-bromothiophene-2-carbaldehyde (250 mg, 1.31 mmol) in place of 5-bromo-2-formylfuran and propylboronic acid (190 mg, 2.16 mmol) in place of hexylboronic acid to give 5-propylthiophene-2-carbaldehyde (58 mg, 29%). Used without further characterization.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09315495B2 |
| 出典データセット | uspto-grants-2016_04 |
| ORD ID | ord-6928120626224b91b3d62cdf9f4537ba |
| 出典メモ | uspto-grants-2016_04 |