4-Bromo-2-methylbenzaldehyde → 2-Methyl-4-butylbenzaldehyde
反応式
[CH3:1][C:2]1[CH:9]=[C:8](Br)[CH:7]=[CH:6][C:3]=1[CH:4]=[O:5].[CH2:11]([B-](F)(F)F)[CH2:12][CH2:13][CH3:14].[K+]>>[CH3:1][C:2]1[CH:9]=[C:8]([CH2:11][CH2:12][CH2:13][CH3:14])[CH:7]=[CH:6][C:3]=1[CH:4]=[O:5]参加物
3
実験手順
The compound was synthesized as in Example 3.1 using 2-methyl-4-bromobenzaldehyde (113 mg, 0.57 mmol) in place of 5-bromo-2-formylfuran and potassium butyltrifluoroborate (113 mg, 0.69 mmol) in place of hexylboronic acid to give 2-methyl-4-butylbenzaldehyde (34 mg, 35%). Used without further characterization.
出典と根拠
- ORDレコード
- ord-eb46a0acf6184148b18cb68e5587639e
- 出典データセット
- uspto-grants-2016_04
- 特許番号
- US09315495B2
反応ノート
読み込み中…