1,2,3-Trichloropropane → 1,1,2,3-Tetrachloro-1-propene

HRID 631758

反応式

HRID 631758 の反応式
ClCC(Cl)CCl.C1C(Cl)=C(Cl)C=C(Cl)C=1OCCO.[Cl:20][CH:21]([Cl:27])[C:22](Cl)([Cl:25])[CH2:23][Cl:24].[Cl:28][C:29]([Cl:35])([Cl:34])[CH:30]([Cl:33])[CH2:31]Cl.ClC(Cl)(Cl)C(Cl)(Cl)C>>[Cl:33][C:30]([C:29]([Cl:35])([Cl:34])[Cl:28])=[CH2:31].[Cl:20][C:21]([Cl:27])=[C:22]([Cl:25])[CH2:23][Cl:24]

参加物

7

反応物 5

HCID 72851,2,3-TrichloropropaneHCID 16462FenteracolHCID 855621,1,2,2,3-PentachloropropaneHCID 186684Propane, pentachloro-HCID 134544911,1,1,2,3-Pentachloropropane

生成物 2

HCID 252811,1,2,3-Tetrachloro-1-propeneHCID 5887421-Propene, 2,3,3,3-tetrachloro-

実験手順

The overhead stream comprising 1,2,3-trichloropropane, TCPE, tetrachloropropanes, 1,1,2,2,3-pentachloropropane, 1,1,1,2,3-pentachloropropane, and 1,1,1,2,2-pentachloropropane is then provided to a reactor where it is dehydrochlorinated to provide dichloropropenes, trichloropropenes, 2,3,3,3-tetrachloropropene, and 1,1,2,3-tetrachloropropene. More specifically, dehydrochlorination reactor may typically be a batch or a continuous stirred tank reactor. The mixing can be done, e.g., by mechanical or jet mixing of feed streams. Those of ordinary skill in the art are readily able to determine the appropriate conditions at which to run a dehydrochlorination reactor in order to conduct the aforementioned dehydrochlorination.

後処理

  1. customis then provided to a reactor where it

出典と根拠

ORDレコード
ord-3982892dfcc3409083277abf43af557c
出典データセット
uspto-grants-2016_04
特許番号
US09321707B2

関連ノート

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