Water → Phenol

HRID 631759

反応式

HRID 631759 の反応式
[CH:1]1([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[OH2:13]>>[C:1]1(=[O:13])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:1]1([OH:13])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:7][CH:12]1[CH2:8][CH2:9][CH2:10][C:11]1=[O:13]

参加物

5

反応物 2

HCID 962WaterHCID 13229Cyclohexylbenzene

生成物 3

HCID 996PhenolHCID 7967CyclohexanoneHCID 142652-Methylcyclopentanone

実験手順

The neutralized cleavage reaction product mixture can then be separated by methods such as distillation. In one example, in a first fractionation column after the cleavage reactor, a heavies fraction comprising the amine salt is obtained at the bottom of the column, a side fraction comprising cyclohexylbenzene is obtained in the middle section, and an upper fraction comprising cyclohexanone, phenol, methylcyclopentanone, and water is obtained.

後処理

  1. customThe neutralized cleavage reaction product mixture can then be separated by methods such as distillation
  2. customis obtained at the bottom of the column
  3. customis obtained in the middle section

出典と根拠

ORDレコード
ord-ca2a3698fec944b89e120b7f0aeaca5d
出典データセット
uspto-grants-2016_04
特許番号
US09321711B2

関連ノート

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