化工社化工社 化学情報印刷レポート · 研究参考用
6-(3-Chloro-phenyl)-5-cyclopropyl-pyridine-2-carboxylic acid → 6-(3-Chloro-phenyl)-5-cyclopropyl-pyridine-2-carboxylic acid (1-ethyl-1-methylcarbamoyl-propyl)-amide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-(3-Chloro-phenyl)-5-cyclopropyl-pyridine-2-carboxylic acid | HCID 71087453 | — |
| 反応物 | 2-Amino-2-ethyl-N-methyl-butyramide | HCID 79810370 | — |
| 生成物 | 6-(3-Chloro-phenyl)-5-cyclopropyl-pyridine-2-carboxylic acid (1-ethyl-1-methylcarbamoyl-propyl)-amide | HCID 71113178 | — |
反応手順
The title compound was synthesized in analogy to Example 1, using 6-(3-chloro-phenyl)-5-cyclopropyl-pyridine-2-carboxylic acid (Example 48 e) and 2-amino-2-ethyl-N-methyl-butyramide (Example 70 b) as starting materials, MS (EI): m/e=400.2 [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09321727B2 |
| 出典データセット | uspto-grants-2016_04 |
| ORD ID | ord-0c8390ad788b41169acb81e8718fcf4e |
| 出典メモ | uspto-grants-2016_04 |