2,4-Diethylthioxanthone → Dipropyleneglycol monomethyl ether

HRID 634567

反応式

HRID 634567 の反応式
[C:1]([OH:5])(=O)[CH:2]=[CH2:3].[C:6]([OH:10])(=O)[CH:7]=[CH2:8].[C:11](O)(=[O:14])C=C.C(C(CO)(CO)CC)O.C(C1C=C(CC)C2SC3C(=CC=CC=3)C(=O)C=2C=1)C>[O-][Ti]([O-])=O.[Ba+2].C(O)C>[CH3:11][O:14][CH:7]([CH2:6][O:10][CH:2]([CH2:1][OH:5])[CH3:3])[CH3:8]

参加物

5

反応物 2

HCID 1228252,4-DiethylthioxanthoneHCID 250191762-Ethyl-2-(hydroxymethyl)propane-1,3-diol;prop-2-enoic acid

生成物 1

HCID 25485Dipropyleneglycol monomethyl ether収率 39.4%

試薬・触媒・溶媒 2

HCID 6101006Barium titanium trioxide触媒HCID 702Ethanol溶媒

実験手順

A slurry obtained by mixing 6.2 g of a borosilicate glass powder, 56.0 g of barium titanate, 6.2 g of an acrylic organic binder containing hydroxyl groups, 3.1 g of ethanol, 3.0 g of trimethylolpropane triacrylate, 1.2 g of 2-methyl-1-[4-(methylthio)phenyl]-2-morphorinopropane-1-on, 0.3 g of 2,4-diethylthioxanthone and 0.5 g of dipropyleneglycol monomethyl ether was formed into a sheet by the doctor blade method. The sheet was dried at 100° C. to obtain a photosensitive dielectric ceramic green sheet with a thickness of 30 μm.

後処理

  1. customA slurry obtained

出典と根拠

ORDレコード
ord-cfa2b1b5def348e7bcd074b938d77348
出典データセット
uspto-grants-2001_02
特許番号
US06183669B2

関連ノート

読み込み中…