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Alanine methyl ester hydrochloride → N-[N-(Phenylacetyl)-L-alaninyl]-L-alanine Methyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Alanine methyl ester hydrochloride | HCID 2733257 | — |
| 反応物 | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| 生成物 | N-[N-(Phenylacetyl)-L-alaninyl]-L-alanine Methyl Ester | HCID 22895047 | — |
反応手順
Following General Procedure A and using N-(phenylacetyl)-L-alanine (from Example B1 above) and L-alanine methyl ester hydrochloride (Aldrich), the title compound was prepared as a solid (mp=140.5-142° C.). The reaction was monitored by tlc (Rf=0.17 in 50% EtOAc/hexanes).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06191166B1 |
| 出典データセット | uspto-grants-2001_02 |
| ORD ID | ord-5f92a0c1cfbb4e75b369e606cf5df4e4 |
| 出典メモ | uspto-grants-2001_02 |