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1,4-Butanedisulfonyl dichloride → 1,4-Benzenedithiol 1,4-butanedisulfonylchloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,4-Butanedisulfonyl dichloride | HCID 315317 | — |
| 反応物 | 1,4-Benzenedithiol | HCID 4691729 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 1,4-Benzenedithiol 1,4-butanedisulfonylchloride | HCID 86756466 | — |
反応手順
Next, the 1,4-butanedisulfonyl chloride vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 15 minutes. Consequently, 1,4-butanedisulfonyl chloride condensed on the surface of the base particles. A polymerization reaction, using as a catalyst triethylamine contained in the base particles, took place between 1,4-butanedisulfonyl chloride condensed on the surface of the base particles and 1,4-benzenedithiol contained therein, forming a film of 1,4-benzenedithiol-1,4-butanedisulfonylchloride co-polymer on the surface of the base particles.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06194487B1 |
| 出典データセット | uspto-grants-2001_02 |
| ORD ID | ord-13f86d582be44e5996ae3030983279a0 |
| 出典メモ | uspto-grants-2001_02 |