2,4-Mesitylenedisulfonyl Dichloride → 2,4-Mesitylenedisulfonylchloride 1,4-benzenedithiol

HRID 636775ノート

反応式

HRID 636775 の反応式
[C:1]1([SH:8])[CH:6]=[CH:5][C:4]([SH:7])=[CH:3][CH:2]=1.[C:9]1([CH3:25])[CH:14]=[C:13]([CH3:15])[C:12]([S:16]([Cl:19])(=[O:18])=[O:17])=[C:11]([CH3:20])[C:10]=1[S:21]([Cl:24])(=[O:23])=[O:22]>>[C:9]1([CH3:25])[CH:14]=[C:13]([CH3:15])[C:12]([S:16]([Cl:19])(=[O:18])=[O:17])=[C:11]([CH3:20])[C:10]=1[S:21]([Cl:24])(=[O:22])=[O:23].[C:1]1([SH:8])[CH:6]=[CH:5][C:4]([SH:7])=[CH:3][CH:2]=1

参加物

3

反応物 2

HCID 36200812,4-Mesitylenedisulfonyl DichlorideHCID 46917291,4-Benzenedithiol2 回

生成物 1

HCID 867564672,4-Mesitylenedisulfonylchloride 1,4-benzenedithiol

実験手順

Next, the 1,4-benzenedithiol vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 30 minutes. Consequently, a further polymerization reaction between 2,4-mesitylenedisulfonyl chloride and 1,4-benzenedithiol took place on the surface of the modified particles (19), forming a film of 2,4-mesitylenedisulfonylchloride-1,4-benzenedithiol co-polymer.

出典と根拠

ORDレコード
ord-e1832136fd6848d2baea10330db99e2c
出典データセット
uspto-grants-2001_02
特許番号
US06194487B1

反応ノート

読み込み中…