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HRID 636776作成日:2026年10月26日

Dabco → Di(2-mercaptoethyl)ether 1,4-butanedisulfonyl chloride

https://huagongshe.com/reaction/636776

反応式

関与物質

役割名称HCID仕込み量
反応物DabcoHCID 9237—
反応物2,2'-OxybisethanethiolHCID 75073—
反応物1,4-Butanedisulfonyl dichlorideHCID 315317—
生成物Di(2-mercaptoethyl)ether 1,4-butanedisulfonyl chlorideHCID 86756468—

反応手順

The base particles, along with helium gas, were cooled and introduced through the particle intake 4 into the vapor atmosphere of 1,4-butanedisulfonyl chloride in the condensing chamber 26. Next, in the mixing section 22, the vapor of 1,4-butanedisulfonyl chloride was cooled, and the introduced base particles were exposed thereto for 10 minutes. Consequently, a polymerization reaction, using as a catalyst triethylenediamine contained in the base particles, took place on the surface of the base particles between di(2-mercaptoethyl)ether and 1,4-butanedisulfonyl chloride, forming a film of di(2-mercaptoethyl)ether-1,4-butanedisulfonyl chloride co-polymer.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06194487B1
出典データセットuspto-grants-2001_02
ORD IDord-c8607af1eb714855bbe19d2842843eca
出典メモuspto-grants-2001_02