化工社化工社 化学情報印刷レポート · 研究参考用
Dabco → Di(2-mercaptoethyl)ether 1,4-butanedisulfonyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dabco | HCID 9237 | — |
| 反応物 | 2,2'-Oxybisethanethiol | HCID 75073 | — |
| 反応物 | 1,4-Butanedisulfonyl dichloride | HCID 315317 | — |
| 生成物 | Di(2-mercaptoethyl)ether 1,4-butanedisulfonyl chloride | HCID 86756468 | — |
反応手順
The base particles, along with helium gas, were cooled and introduced through the particle intake 4 into the vapor atmosphere of 1,4-butanedisulfonyl chloride in the condensing chamber 26. Next, in the mixing section 22, the vapor of 1,4-butanedisulfonyl chloride was cooled, and the introduced base particles were exposed thereto for 10 minutes. Consequently, a polymerization reaction, using as a catalyst triethylenediamine contained in the base particles, took place on the surface of the base particles between di(2-mercaptoethyl)ether and 1,4-butanedisulfonyl chloride, forming a film of di(2-mercaptoethyl)ether-1,4-butanedisulfonyl chloride co-polymer.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06194487B1 |
| 出典データセット | uspto-grants-2001_02 |
| ORD ID | ord-c8607af1eb714855bbe19d2842843eca |
| 出典メモ | uspto-grants-2001_02 |