化工社化工社 化学情報印刷レポート · 研究参考用
1,6-Hexanediol → 1,6-Hexanediol adipoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,6-Hexanediol | HCID 12374 | — |
| 反応物 | Adipoyl chloride | HCID 61034 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 1,6-Hexanediol adipoyl chloride | HCID 86756475 | — |
反応手順
Next, the adipoyl chloride vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 3 minutes. Consequently, adipoyl chloride condensed on the surface of the base particles. A polymerization reaction, using as a catalyst triethylamine contained in the base particles, took place between adipoyl chloride condensed on the surface of the base particles and 1,6-hexanediol contained therein, forming a film of 1,6-hexanediol-adipoyl chloride co-polymer on the surface of the base particles.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06194487B1 |
| 出典データセット | uspto-grants-2001_02 |
| ORD ID | ord-7d3f9ba074624e8a96aaeab24379b4c5 |
| 出典メモ | uspto-grants-2001_02 |