化工社化工社 化学情報印刷レポート · 研究参考用
Terephthaloyl chloride → 1,4-Butanedithiol terephthaloyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Terephthaloyl chloride | HCID 7488 | — |
| 反応物 | 1,4-Butanedithiol | HCID 79148 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 1,4-Butanedithiol terephthaloyl chloride | HCID 86756479 | — |
反応手順
Next, the terephthaloyl chloride vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 3 minutes. Consequently, terephthaloyl chloride condensed on the surface of the base particles. A polymerization reaction, using as a catalyst triethylamine, took place between terephthaloyl chloride condensed on the surface of the base particles and 1,4-butanedithiol contained therein, forming a film of 1,4-butanedithiol-terephthaloyl chloride co-polymer on the surface of the base particles.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06194487B1 |
| 出典データセット | uspto-grants-2001_02 |
| ORD ID | ord-eb1a8c24168c465095dacc02a977c997 |
| 出典メモ | uspto-grants-2001_02 |