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4-(1-Imidazolyl)benzoic Acid → Carbon Dioxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(1-Imidazolyl)benzoic Acid | HCID 736529 | — |
| 反応物 | 5-Ethyl-2,3-dihydro-2-oxo-1H-imidazole-4-carboxylic acid | HCID 13815989 | — |
| 溶媒 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | Carbon Dioxide | HCID 280 | — |
| 生成物 | CK 2289 | HCID 127769 | — |
反応手順
In a manner similar to that described in Example IA react 5-ethyl-2,3-dihydro-2-oxo-1H-imidazole-4-carboxylic acid and 4-(1H-imidazol-1-yl)benzoic acid, dissolve the crude free base in aqueous sodium hydroxide and reprecipitate with carbon dioxide to produce the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04556665 |
| 出典データセット | uspto-grants-1985_12 |
| ORD ID | ord-bb69656e41b64be39d5500152f332783 |
| 出典メモ | uspto-grants-1985_12 |