Formamide → Penconazole
反応式
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]([CH2:17][CH2:18][CH3:19])[CH2:10][N:11]([CH:15]=O)[NH:12][CH:13]=O.C([NH2:22])=O>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]([CH2:17][CH2:18][CH3:19])[CH2:10][N:11]1[CH:15]=[N:22][CH:13]=[N:12]1参加物
3
実験手順
6.2 g of the 1-[2-(2,4-dichlorophenyl)-pentyl-1,2-diformylhydrazine obtained according to Example 14 are heated, without purification, in 50 ml of formamide at 170° C. for 6 hours. Chromatography of the product obtained yields 1-[2-(2,4-dichlorophenyl)-pentyl]-1H-1,2,4-triazole, the 1H-NMR spectrum of which agrees with the 1H-NMR spectrum of the same compound described in Example 12.
後処理
- customChromatography of the product obtained
出典と根拠
- ORDレコード
- ord-11d8ef2b707a44308120a68f7f44cd06
- 出典データセット
- uspto-grants-1985_12
- 特許番号
- US04556717
反応ノート
読み込み中…