化工社化工社 化学情報印刷レポート · 研究参考用
N-[(Phenylmethoxy)carbonyl]-L-isoleucine → Ethyl N-Carbobenzyloxy-L-isoleucyl-N-(3-pyridyl)glycinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-[(Phenylmethoxy)carbonyl]-L-isoleucine | HCID 2724772 | — |
| 反応物 | ethyl N-(3-pyridyl)-glycinate | HCID 20255549 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Ethyl N-Carbobenzyloxy-L-isoleucyl-N-(3-pyridyl)glycinate | HCID 54257317 | — |
反応手順
A methylene chloride solution of N-carbobenzyloxy-L-isoleucine and ethyl N-(3-pyridyl)-glycinate was treated with N,N-dicyclohexylcarbodiimide as in example 5A. Purification of the product was accomplished by chromatography on silica-gel.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04558038 |
| 出典データセット | uspto-grants-1985_12 |
| ORD ID | ord-a1fdac81623e4d5791d08979bc3bd5fa |
| 出典メモ | uspto-grants-1985_12 |