Dimethylformamide dimethyl acetal → 2(1H)-Pyridinone, 5-acetyl-6-[2-(dimethylamino)ethenyl]-

反応式

[C:1]([C:4]1[CH:5]=[CH:6][C:7](=[O:11])[NH:8][C:9]=1[CH3:10])(=[O:3])[CH3:2].CO[CH:14](OC)[N:15]([CH3:17])[CH3:16]>>[C:1]([C:4]1[CH:5]=[CH:6][C:7](=[O:11])[NH:8][C:9]=1[CH:10]=[CH:14][N:15]([CH3:17])[CH3:16])(=[O:3])[CH3:2]

参加物

反応物 2

HCID 78373Dimethylformamide dimethyl acetal

HCID 44217365-acetyl-6-methyl-2(1H)-pyridinone

生成物 1

HCID 37350622(1H)-Pyridinone, 5-acetyl-6-[2-(dimethylamino)ethenyl]-

実験手順

The process according to claim 9 which comprises reacting 5-acetyl-6-methyl-2(1H)-pyridinone with dimethylformamide dimethyl acetal to produce 5-acetyl-6-(2-dimethylaminoethenyl)-2(1H)-pyridinone.

出典と根拠

ORDレコード: ord-db9f14ec2bb84e11bb8e37743ac3424b
出典データセット: uspto-grants-1985_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04559347

反応ノート

読み込み中…