Methyl 3-(hex-3-en-1-yl)-4,5-dimethoxybenzoate → Methyl 3-hexyl-4,5-dimethoxybenzoate

HRID 638920ノート

反応式

HRID 638920 の反応式
[CH3:1][O:2][C:3](=[O:20])[C:4]1[CH:9]=[C:8]([O:10][CH3:11])[C:7]([O:12][CH3:13])=[C:6]([CH2:14][CH2:15][CH:16]=[CH:17][CH2:18][CH3:19])[CH:5]=1>CCOC(C)=O>[CH3:1][O:2][C:3](=[O:20])[C:4]1[CH:9]=[C:8]([O:10][CH3:11])[C:7]([O:12][CH3:13])=[C:6]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])[CH:5]=1

参加物

3

反応物 1

HCID 68684188Methyl 3-(hex-3-en-1-yl)-4,5-dimethoxybenzoate

生成物 1

HCID 68685356Methyl 3-hexyl-4,5-dimethoxybenzoate

試薬・触媒・溶媒 1

HCID 8857Ethyl Acetate溶媒

実験手順

3-Hexyl-4,5-dimethoxybenzoic acid methyl ester was prepared from 3-hex-3-enyl-4,5-dimethoxybenzoic acid methyl ester by following Method H using EtOAc as a solvent. The reaction was conducted for 2.5 h under hydrogen atmosphere. The product obtained in quantitative yield was used without further purification.

後処理

  1. customThe product obtained in quantitative yield
  2. customwas used without further purification

出典と根拠

ORDレコード
ord-d6e16dcf34144d11a431166a278f78a2
出典データセット
uspto-grants-2010_04
特許番号
US07691843B2

反応ノート

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