Methyl 3,4-dimethoxy-5-(pent-3-en-1-yl)benzoate → Methyl 3,4-dimethoxy-5-pentylbenzoate
反応式
[CH3:1][O:2][C:3](=[O:19])[C:4]1[CH:9]=[C:8]([CH2:10][CH2:11][CH:12]=[CH:13][CH3:14])[C:7]([O:15][CH3:16])=[C:6]([O:17][CH3:18])[CH:5]=1>CCOC(C)=O>[CH3:1][O:2][C:3](=[O:19])[C:4]1[CH:9]=[C:8]([CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[C:7]([O:15][CH3:16])=[C:6]([O:17][CH3:18])[CH:5]=1参加物
3
実験手順
3,4-Dimethoxy-5-pentylbenzoic acid methyl ester was prepared 3,4-dimethoxy-5-pent-3-enylbenzoic methyl ester by following Method H using EtOAc as a solvent. The reaction was conducted for 2.5 h under hydrogen atmosphere. The product, obtained in quantitative yield, was used without further purification.
後処理
- customThe product, obtained in quantitative yield
- customwas used without further purification
出典と根拠
- ORDレコード
- ord-f43dd26c80b349c5907b3fa0f83b87bc
- 出典データセット
- uspto-grants-2010_04
- 特許番号
- US07691843B2
反応ノート
読み込み中…