化工社化工社 化学情報印刷レポート · 研究参考用
Allyl bromide → 4-Allyloxy-3-allylbenzoic acid methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Allyl bromide | HCID 7841 | — |
| 反応物 | Methyl 3-allyl-4-hydroxybenzoate | HCID 939882 | — |
| 生成物 | 4-Allyloxy-3-allylbenzoic acid methyl ester | HCID 11241748 | 93% |
反応手順
4-Allyloxy-3-allylbenzoic acid methyl ester was prepared by reacting 3-allyl-4-hydroxybenzoic acid methyl ester (Example 49, Step 2) with allyl bromide following Method C in 93% yield. The reaction was conducted at room temperature for 16 h and the resulting product was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07691843B2 |
| 出典データセット | uspto-grants-2010_04 |
| ORD ID | ord-f4c296dd85584bfd8976809853a8fb26 |
| 出典メモ | uspto-grants-2010_04 |