Allyl bromide → 4-Allyloxy-3-allylbenzoic acid methyl ester

HRID 638949

反応式

HRID 638949 の反応式
[CH3:1][O:2][C:3](=[O:14])[C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[C:6]([CH2:11][CH:12]=[CH2:13])[CH:5]=1.[CH2:15](Br)[CH:16]=[CH2:17]>>[CH3:1][O:2][C:3](=[O:14])[C:4]1[CH:9]=[CH:8][C:7]([O:10][CH2:17][CH:16]=[CH2:15])=[C:6]([CH2:11][CH:12]=[CH2:13])[CH:5]=1

参加物

3

反応物 2

HCID 7841Allyl bromideHCID 939882Methyl 3-allyl-4-hydroxybenzoate

生成物 1

HCID 112417484-Allyloxy-3-allylbenzoic acid methyl ester収率 93%

実験手順

4-Allyloxy-3-allylbenzoic acid methyl ester was prepared by reacting 3-allyl-4-hydroxybenzoic acid methyl ester (Example 49, Step 2) with allyl bromide following Method C in 93% yield. The reaction was conducted at room temperature for 16 h and the resulting product was used without further purification.

後処理

  1. customthe resulting product was used without further purification

出典と根拠

ORDレコード
ord-f4c296dd85584bfd8976809853a8fb26
出典データセット
uspto-grants-2010_04
特許番号
US07691843B2

関連ノート

読み込み中…