3-Methoxybenzoic Acid → Benzoic acid, 3-methoxy-, ethyl ester
反応式
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6]([OH:8])=[O:7].[CH2:12](O)[CH3:13].OS(O)(=O)=O>>[CH2:12]([O:7][C:6](=[O:8])[C:5]1[CH:9]=[CH:10][CH:11]=[C:3]([O:2][CH3:1])[CH:4]=1)[CH3:13]参加物
3
実験手順
3-Methoxy-benzoic acid ethyl ester is prepared from 3-methoxy-benzoic acid using a standard protocol with ethanol/H2SO4 according to L.-F. Tietze & T. Eicher, Reactions and Syntheses in the Organic Chemistry Laboratory; University Science Books, Mill Valley, Calif., 1989). Title compound: b.p. 151° C. (25 mm Hg); single peak at tR=6.51 min (System 1).
出典と根拠
- ORDレコード
- ord-e76a92e869664f87b1dcedd07a530cc2
- 出典データセット
- uspto-grants-2010_04
- 特許番号
- US07691855B2
反応ノート
読み込み中…