化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl Acrylate → HCID 15696577、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl Acrylate | HCID 8821 | — |
| 反応物 | Ethyl 3-aminobutyrate | HCID 98103 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 15696577 | HCID 15696577 | — |
反応手順
A solution of ethyl 3-aminobutanoate (4.2 g) and of ethyl 2-propenoate (3.83 mL) in EtOH (20 mL) was stirred at room temperature for 8 h. The solvent was evaporated under reduced pressure and the residue purified by chromatography on NH column eluting with a gradient from 100% cyclohexane to 90% ethyl acetate/cyclohexane. The title compound was isolated as a colourless oil, 3.9 g (MS (m/z): 232 [MH]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07691893B2 |
| 出典データセット | uspto-grants-2010_04 |
| ORD ID | ord-266854fc87104b09ac26d16514c66928 |
| 出典メモ | uspto-grants-2010_04 |