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ethyl 2-methyl-1H-indole-3-carboxylate → 2-Methyl-1-phenyl-1H-indole-3-carboxylic acid ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | ethyl 2-methyl-1H-indole-3-carboxylate | HCID 4072358 | — |
| 反応物 | Ethyl 2-methyl-1-phenyl-1H-pyrrole-3-carboxylate | HCID 15272135 | — |
| 生成物 | 2-Methyl-1-phenyl-1H-indole-3-carboxylic acid ethyl ester | HCID 15953410 | — |
反応手順
Prepared in analogy to that of 2-methyl-1-phenyl-1H-pyrrole-3-carboxylic acid ethyl ester from 2-Methyl-1H-indole-3-carboxylic acid ethyl ester. The title compound, 1H NMR (200 MHz, CDCl3): δ (ppm)=8.15 (d, 1H, J=7.4 Hz), 7.6-6.9 (m, 8H), 4.43 (q, 2H, J=7.4 Hz), 2.59 (s, 3H), 1.47 (t, 3H, J=7.4 Hz).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07696223B2 |
| 出典データセット | uspto-grants-2010_04 |
| ORD ID | ord-077312ff0a8743a7abee8be20c68df7b |
| 出典メモ | uspto-grants-2010_04 |