1-(Bromomethyl)naphthalene → HCID 58900296、化合物

反応式

C[O:2][C:3]([C:5]1[NH:6][C:7]2[C:12]([C:13]=1[C:14]([O:16]C)=[O:15])=[CH:11][CH:10]=[CH:9][CH:8]=2)=[O:4].Br[CH2:19][C:20]1[C:29]2[C:24](=[CH:25][CH:26]=[CH:27][CH:28]=2)[CH:23]=[CH:22][CH:21]=1>>[C:20]1([CH2:19][N:6]2[C:7]3[C:12](=[CH:11][CH:10]=[CH:9][CH:8]=3)[C:13]([C:14]([OH:16])=[O:15])=[C:5]2[C:3]([OH:2])=[O:4])[C:29]2[C:24](=[CH:25][CH:26]=[CH:27][CH:28]=2)[CH:23]=[CH:22][CH:21]=1

参加物

反応物 2

HCID 1378441-(Bromomethyl)naphthalene

HCID 143197Dimethyl indole-2,3-dicarboxylate

生成物 1

HCID 58900296HCID 58900296、化合物

実験手順

Using general procedure B, 1H-indole-2,3-dicarboxylic acid dimethyl ester was coupled with 1-bromomethyl-naphthalene and the product obtained was hydrolyzed to give the title compound as a white solid. MS: 344.3 ([M−H]−).

後処理

customthe product obtained

出典と根拠

ORDレコード: ord-91a6b53651064cc883d52ff422b903fa
出典データセット: uspto-grants-2010_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07696240B2

反応ノート

読み込み中…