化工社化工社 化学情報印刷レポート · 研究参考用
Cyclohexylamine → 8-Methylnonanoic acid cyclohexylamine salt
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexylamine | HCID 7965 | — |
| 反応物 | 8-Methylnonanoic acid | HCID 111470 | — |
| 溶媒 | Heptane | HCID 8900 | — |
| 生成物 | 8-Methylnonanoic acid cyclohexylamine salt | HCID 68605324 | — |
反応手順
From the 8-methylnonanoic acid crude product obtained in Example 1, 8.00 g was dissolved in heptane (30 ml). Cyclohexylamine (6.91 ml, 60.4 mmol) was slowly added dropwise at 0° C. (ice bath), and the mixture was stirred at room temperature for 20 minutes. The reaction mixture was filtered to give 8-methylnonanoic acid cyclohexylamine salt (15.7 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07700331B2 |
| 出典データセット | uspto-grants-2010_04 |
| ORD ID | ord-f0e91b54879e4f9caeab73e5e708080f |
| 出典メモ | uspto-grants-2010_04 |