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HRID 643199作成日:2026年10月24日

Cyclohexylamine → 8-Methylnonanoic acid cyclohexylamine salt

https://huagongshe.com/ja/reaction/643199

反応式

関与物質

役割名称HCID仕込み量
反応物CyclohexylamineHCID 7965—
反応物8-Methylnonanoic acidHCID 111470—
溶媒HeptaneHCID 8900—
生成物8-Methylnonanoic acid cyclohexylamine saltHCID 68605324—

反応手順

From the 8-methylnonanoic acid crude product obtained in Example 1, 8.00 g was dissolved in heptane (30 ml). Cyclohexylamine (6.91 ml, 60.4 mmol) was slowly added dropwise at 0° C. (ice bath), and the mixture was stirred at room temperature for 20 minutes. The reaction mixture was filtered to give 8-methylnonanoic acid cyclohexylamine salt (15.7 g).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07700331B2
出典データセットuspto-grants-2010_04
ORD IDord-f0e91b54879e4f9caeab73e5e708080f
出典メモuspto-grants-2010_04