2,5-Dimethylbenzaldehyde → [3-(8-Chloro-3-phenylcinnolin-4-yl)phenyl](2,5-dimethylbenzyl)amine

反応式

[Cl:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:11]=1[N:10]=[N:9][C:8]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)=[C:7]2[C:18]1[CH:19]=[C:20]([NH2:24])[CH:21]=[CH:22][CH:23]=1.[CH3:25][C:26]1[CH:33]=[CH:32][C:31]([CH3:34])=[CH:30][C:27]=1[CH:28]=O>>[Cl:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:11]=1[N:10]=[N:9][C:8]([C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1)=[C:7]2[C:18]1[CH:19]=[C:20]([NH:24][CH2:28][C:27]2[CH:30]=[C:31]([CH3:34])[CH:32]=[CH:33][C:26]=2[CH3:25])[CH:21]=[CH:22][CH:23]=1

参加物

反応物 2

HCID 220152,5-Dimethylbenzaldehyde

HCID 118566993-(8-Chloro-3-phenyl-cinnolin-4-yl)-phenylamine

生成物 1

HCID 11856162[3-(8-Chloro-3-phenylcinnolin-4-yl)phenyl](2,5-dimethylbenzyl)amine

実験手順

The title compound was prepared from 3-(8-chloro-3-phenyl-cinnolin-4-yl)-phenylamine and 2,5-dimethylbenzaldehyde according to the procedure of Step 5 Example 6. MS (ES) m/z 450.2.

出典と根拠

ORDレコード: ord-ce481de9fc6a4f30832324ccc5ce58ef
出典データセット: uspto-grants-2010_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07700595B2

反応ノート

読み込み中…