化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Acid → 2-(4-Aminophenoxy)-2-methylpropanoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | 2-(4-Acetamidophenoxy)-2-methylpropanoic acid | HCID 14879855 | — |
| 溶媒 | Potassium Hydroxide | HCID 14797 | — |
| 生成物 | 2-(4-Aminophenoxy)-2-methylpropanoic acid | HCID 2774958 | 62% |
反応手順
1.18 g (0.005 mol) of the 2-(4-acetaminophenoxy)-2-methyl propionic acid is boiled in 10% KOH (60 ml) for 1/2 hour. The solution is then cooled and acidified with acetic acid to yield 0.6 g (62% yield) of 2-(4-aminophenoxy)-2-methyl propionic acid as a yellowish white powder, mp 214°-16° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05248785 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-13b9f603fcc84708924f96e5ef9dda01 |
| 出典メモ | uspto-grants-1993_09 |