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Pyridine → Allyl 2-[4-(2-quinoxalinyloxy)phenoxy]propanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pyridine | HCID 1049 | — |
| 反応物 | Allyl Alcohol | HCID 7858 | — |
| 反応物 | 2-[4-(2-Quinoxalinyloxy)phenoxy]propionyl chloride | HCID 13670532 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Allyl 2-[4-(2-quinoxalinyloxy)phenoxy]propanoate | HCID 13670534 | — |
反応手順
To a solution of 1.2 g allyl alcohol and 1.6 g pyridine in 50 cc methylene chloride, add 6.6 g of 2-[4-(2-quinoxalinyloxy)phenoxy]propionyl chloride in 60 cc methylene chloride. Stir the mixture at room temperature overnight. Wash the methylene chloride solution with water and dry the solution over magnesium sulfate concentrate under vacuum to give allyl 2-[4-(2-quinoxalinyloxy)phenoxy]propanoate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04609396 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-a9135ae31a7f4357adf017005813a8cd |
| 出典メモ | uspto-grants-1986_09 |