化工社化工社 化学情報印刷レポート · 研究参考用
2-Methylcyclopentanone → N-Methyl-6-{[3-(2-methylcyclopentyl)-2,3,4,5-tetrahydro-1H-3-benzazepin-7-yl]oxy}-3-pyridinecarboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methylcyclopentanone | HCID 14265 | — |
| 反応物 | N-Methyl-6-(2,3,4,5-tetrahydro-1H-3-benzazepin-7-yloxy)-3-pyridinecarboxamide | HCID 57440288 | — |
| 生成物 | N-Methyl-6-{[3-(2-methylcyclopentyl)-2,3,4,5-tetrahydro-1H-3-benzazepin-7-yl]oxy}-3-pyridinecarboxamide | HCID 10429809 | — |
反応手順
Example 224 (E224) was prepared from N-methyl-6-(2,3,4,5-tetrahydro-1H-3-benzazepin-7-yloxy)-3-pyridinecarboxamide (D40) and 2-methyl cyclopentanone using the method described for Example 223; MS (ES+) m/e 380 [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07704994B2 |
| 出典データセット | uspto-grants-2010_04 |
| ORD ID | ord-c3a0ae3fba704378997754d080ca4092 |
| 出典メモ | uspto-grants-2010_04 |