Benzaldehyde → HCID 25050877、化合物

HRID 646056ノート

反応式

HRID 646056 の反応式
[CH3:1][C:2]1([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[C:5](=[O:6])[CH2:4][C:3]1=[O:7].[CH:14](=O)[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.[CH3:22][C:23]([NH:36][C:37](=[O:39])[CH3:38])([CH3:35])[CH2:24][C:25]1[C:33]2[C:28](=[CH:29][C:30]([CH3:34])=[CH:31][CH:32]=2)[NH:27][CH:26]=1>>[OH:6][C:5]1[C:2]([CH3:1])([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[C:3](=[O:7])[C:4]=1[CH:14]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)[C:26]1[NH:27][C:28]2[C:33]([C:25]=1[CH2:24][C:23]([NH:36][C:37](=[O:39])[CH3:38])([CH3:22])[CH3:35])=[CH:32][CH:31]=[C:30]([CH3:34])[CH:29]=2

参加物

4

反応物 3

HCID 240BenzaldehydeHCID 68580747N-[1,1-dimethyl-2-(6-methyl-1H-indol-3-yl)-ethyl]-acetamideHCID 685810272-Methyl-2-phenyl-cyclobutane-1,3-dione

生成物 1

HCID 25050877HCID 25050877、化合物

実験手順

Using general procedure C, 2-methyl-2-phenyl-cyclobutane-1,3-dione (Lit. 1) was reacted with benzaldehyde and N-[1,1-dimethyl-2-(6-methyl-1H-indol-3-yl)-ethyl]-acetamide (from Example 1.2) to give the title compound as a pale yellow solid. MS: 505.5 ([M−H]−).

出典と根拠

ORDレコード
ord-6eb506636719462385ca44d02d69a565
出典データセット
uspto-grants-2010_04
特許番号
US07705034B2

反応ノート

読み込み中…