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Benzaldehyde → 2-[(3,5-Dimethyl-1H-indol-2-yl)-phenyl-methyl]-3-hydroxy-4-methyl-4-phenyl-cyclobut-2-enone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | 3,5-Dimethylindole | HCID 98615 | — |
| 反応物 | 2-Methyl-2-phenyl-cyclobutane-1,3-dione | HCID 68581027 | — |
| 生成物 | 2-[(3,5-Dimethyl-1H-indol-2-yl)-phenyl-methyl]-3-hydroxy-4-methyl-4-phenyl-cyclobut-2-enone | HCID 25050879 | — |
反応手順
Using general procedure C, 2-methyl-2-phenyl-cyclobutane-1,3-dione (Lit. 1) was reacted with benzaldehyde and 3,5-dimethyl-1H-indole (Lit. 3) to give the title compound as a colorless solid. MS: 406.5 ([M−H]−).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07705034B2 |
| 出典データセット | uspto-grants-2010_04 |
| ORD ID | ord-2aedb6d4798f470892b895736560a396 |
| 出典メモ | uspto-grants-2010_04 |