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Benzaldehyde → 2-Propenoic acid, 3-phenyl-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | Ketene | HCID 10038 | — |
| 反応物 | Sodium Acetate | HCID 517045 | — |
| 生成物 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | 40% |
反応手順
The reaction of benzaldehyde with ketene at 60° C. with the addition of sodium acetate and subsequent heating of the reaction product to the boiling point is known from Ind. Chem. 41, 768 (1949). Cinnamic acid is thereby obtained in a yield of 40%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04609756 |
| 出典データセット | uspto-grants-1986_09 |
| ORD ID | ord-3efb0e77182446a889f8d3914b9a0ea6 |
| 出典メモ | uspto-grants-1986_09 |