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Vinyl isocyanate → HCID 12573482、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Vinyl isocyanate | HCID 77094 | — |
| 反応物 | (1-Chloroethyl)carbamyl chloride | HCID 12573467 | — |
| 溶媒 | 1-Chloronaphthalene | HCID 7003 | — |
| 生成物 | Vinyl isocyanate | HCID 77094 | 8% |
| 生成物 | HCID 12573482 | HCID 12573482 | 92% |
反応手順
30 parts of 1-chloroethylcarbamyl chloride are dissolved in 100 parts by volume of 1-chloronaphthalene and a solution of 16 parts of vinyl isocyanate in 20 parts by volume of 1-chloronaphthalene is added to the mixture in the course of 0.3 hour at 2° C. 12.5 parts (8% of theory) of vinyl isocyanate and 43 parts (92% of theory) of 1-chloroethyl isocyanate are obtained, the determinations being carried out by gas chromatography.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04411752 |
| 出典データセット | uspto-grants-1983_10 |
| ORD ID | ord-15907a3c4348420e97db91a68b610441 |
| 出典メモ | uspto-grants-1983_10 |