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Potassium Hydroxide → Diepoxyoctane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 1,2:7,8-Diepoxyoctane | HCID 17048 | — |
| 生成物 | Diepoxyoctane | HCID 21943853 | — |
反応手順
A 1-liter resin flask was charged with 200 g of PEG-7500 and 0.3 g KOH and vacuum stripped at 100° C. for one-half hour. To this stirred solution under nitrogen were added 5.5 g of 1,2,7,8-diepoxyoctane at 100° C. over 15 minutes. The mixture was maintained at this temperature for an additional one and one-half hours followed by quenching with 250 g of water.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04411775 |
| 出典データセット | uspto-grants-1983_10 |
| ORD ID | ord-8891115a7a3b41ce8053755280664e69 |
| 出典メモ | uspto-grants-1983_10 |