Hydrogen Peroxide → N,N-Dimethylheptylamine N-oxide hydrate

反応式

[CH3:1][N:2]([CH3:10])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].[OH:11]O>>[CH3:1][N+:2]([O-:11])([CH3:10])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]

参加物

反応物 2

HCID 784Hydrogen Peroxide

HCID 16226N,N-Dimethylheptylamine

生成物 1

HCID 5189203N,N-Dimethylheptylamine N-oxide hydrate

実験手順

To 28.6 g of dimethylheptyl amine was added slowly 100 ml 30% H2O2 as in Example 4 to give the dimethylheptyl amine oxide. NMR showed the resulting semisolid material to contain 29% water and 71% of the amine oxide.

出典と根拠

ORDレコード: ord-752520db35a84cba98bc9968885876b5
出典データセット: uspto-grants-1983_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04411893

反応ノート

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